Intervention Studies for the metabolite Hesperetin-3'-sulfate with food phytochemical Orange flavanones

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	Food Phytochemical		Metabolite	Species	Biofluids	Origin	Dietary Source Description	Dietary Source Classification	Total Number of Subjects	Description of Population	Ingested Amount	Single/Multiple Dose	Duration of the Study	Tmax (h)	Cmax (nM)	AUC (nM/h)	Time covered by AUC (h)	t 1/2 (h)	% of 24h Urinary Excretion	Excreted Amount & Time Interval	Publications

	Food Phytochemical		Metabolite	Species	Biofluids	Origin	Dietary Source Description	Dietary Source Classification	Total Number of Subjects	Description of Population	Ingested Amount	Single/Multiple Dose	Duration of the Study	Tmax (h)	Cmax (nM)	AUC (nM/h)	Time covered by AUC (h)	t 1/2 (h)	% of 24h Urinary Excretion	Excreted Amount & Time Interval	Publications
	Orange flavanones		Hesperetin-3'-sulfate	Human	Urine	Host metabolism	350 mL Orange juice with 1 g B. longum R0175	food	15	Healthy; BMI= 18-35 kg/m²	169 µmol flavanones	Single							4.26 (SEM)	7.2 µmol (SEM) (0-24h)	Publications
	Orange flavanones		Hesperetin-3'-sulfate	Human	Urine	Host metabolism	350 mL Orange juice (after 1 g B. longum R0175 1 month)	food	15	Healthy; BMI= 18-35 kg/m²	169 µmol flavanones	Single							6.44 (SEM)	10.9 µmol (SEM) (0-24h)	Publications
	Orange flavanones		Hesperetin-3'-sulfate	Human	Plasma	Host metabolism	500 mL Orange juice (Tropicana with bits)	food	10	Endurance trained; M; Age= 31.8 ± 5.7; BMI= 21.7 ± 1.8 kg/m2	330 μmol flavanones µmol	Single		5.9±0.4 (SEM)	80±24 (SEM)	280	0-8 h				Publications
	Orange flavanones		Hesperetin-3'-sulfate	Human	Urine	Host metabolism	502 mL Orange juice (Tropicana with bits)	food	10	Endurance-trained; M; BMI= 21.7 ± 0.6 kg/m²; performed 5-10 h endurance training per week	330 µmol flavanones	Single							0.51 (SEM)	1.7 µmol (SEM) (0-24h)	Publications
	Orange flavanones		Hesperetin-3'-sulfate	Human	Urine	Host metabolism	503 mL Orange juice (Tropicana with bits)	food	10	Endurance-trained; M; BMI= 21.7 ± 0.6 kg/m²; stoping training for 7 days	330 µmol flavanones	Single							0.72 (SEM)	2.4 µmol (SEM) (0-24h)	Publications
	Orange flavanones		Hesperetin-3'-sulfate	Human	Urine	Host metabolism	250 ml of orange juice	food	4	Healthy ; 2 M;2F; Age=23-30 ; BMI= 19.9-23.5kg/m²	54.09 μmol	Single							0.35	189 nmol (SD) (0-24h)	Publications
	Orange flavanones		Hesperetin-3'-sulfate	Human	Urine	Host metabolism	250 ml pulp enriched orange juice	food	12	Healthy; 6M;6F; Age=23-60;BMI=23.9- 37.2 kg/m²	537 µmol flavanones [naringenin-7-O-rutinoside (114 µmol), hesperetin-7-O-rutinoside (329 µmol), didymin(19 µmol), naringenin-7-O-rutinoside-4'-O-glucoside (51 µmol); hesperetin-7-O-rutinoside-3'-Oglucoside (19 µmol), eriodictyol-7-O-rutinoside (5 µmol)]	Single	24h						5.23	18.2	Publications
	Orange flavanones		Hesperetin-3'-sulfate	Human	Plasma; Urine	Host metabolism	500 ml of orange juice	food	12	Healthy; M; Age=31.8±5.7; BMI=21.7±1.8kg/m²	250µmol of hesperetin derivatives and 75µmol of naringenin derivatives	Single	24h								Publications
	Orange flavanones		Hesperetin-3'-sulfate	Human	Plasma	Host metabolism	500 mL Orange juice (Tropicana with bits)	food	10	Endurance trained; M; Age= 31.8 ± 5.7; BMI= 21.7 ± 1.8 kg/m2	330 μmol flavanones µmol	Single		5.9±0.4 (SEM)	80±24 (SEM)	280	0-8 h				Publications
	Orange flavanones		Hesperetin-3'-sulfate	Human	Urine	Host metabolism	250 ml pulp enriched orange juice	food	12	Healthy; 6M;6F; Age=23-60;BMI=23.9- 37.2 kg/m²	537 µmol flavanones [naringenin-7-O-rutinoside (114 µmol), hesperetin-7-O-rutinoside (329 µmol), didymin(19 µmol), naringenin-7-O-rutinoside-4'-O-glucoside (51 µmol); hesperetin-7-O-rutinoside-3'-Oglucoside (19 µmol), eriodictyol-7-O-rutinoside (5 µmol)]	Single	24h						5,229885057	18,2±7,3	Publications

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